Structural and Functional Characterization of PAA Hydrolase PAAH-2

Location

Presentation- College of Science and Mathematics

Document Type and Release Option

Thesis Presentation (Archived)

Faculty Mentor

Dr. Mitch Weiland

Faculty Mentor Email

mweiland@georgiasouthern.edu

Presentation Year

2021

Start Date

26-4-2021 12:00 AM

End Date

30-4-2021 12:00 AM

Keywords

Georgia Southern University, Honors Symposium, Presentation

Description

Poly(carboxylate), a water-soluble polymer, has many applications, one of which is as a superabsorbent material commonly found in products like diapers and feminine hygiene products. These materials are non-biodegradable and alternatives are necessary to mitigate their accumulation in the environment. Poly(aspartic acid) (PAA) is a safe, biodegradable alternative that can be broken down by three different enzymes. This project focuses on PAAH-2, one of the PAA degrading enzymes, and aims to characterize the catalytic active site of the hydrolase. The DNA sequence for the protein was purchased and then expressed using E. coli cells. The protein was purified using an immobilized metal affinity column and the purity was assessed using SDS-PAGE. Initial crystallization leads were identified by the Hauptmann-Woodward Institute (HWI) and PAAH-2 crystallization experiments were optimized using the conditions initially seen by HWI. Here we will present the structure of PAAH-2 predicted from the crystal structure as well as the activity assays used to characterize the protein.

Academic Unit

College of Science and Mathematics

Comments

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Apr 26th, 12:00 AM Apr 30th, 12:00 AM

Structural and Functional Characterization of PAA Hydrolase PAAH-2

Presentation- College of Science and Mathematics

Poly(carboxylate), a water-soluble polymer, has many applications, one of which is as a superabsorbent material commonly found in products like diapers and feminine hygiene products. These materials are non-biodegradable and alternatives are necessary to mitigate their accumulation in the environment. Poly(aspartic acid) (PAA) is a safe, biodegradable alternative that can be broken down by three different enzymes. This project focuses on PAAH-2, one of the PAA degrading enzymes, and aims to characterize the catalytic active site of the hydrolase. The DNA sequence for the protein was purchased and then expressed using E. coli cells. The protein was purified using an immobilized metal affinity column and the purity was assessed using SDS-PAGE. Initial crystallization leads were identified by the Hauptmann-Woodward Institute (HWI) and PAAH-2 crystallization experiments were optimized using the conditions initially seen by HWI. Here we will present the structure of PAAH-2 predicted from the crystal structure as well as the activity assays used to characterize the protein.